Modernized Liquid Helium-Free Closed-Cycle Cryostat for Mössbauer Research

S. S. Starchikov; Старчиков С. С.; K. O. Funtov; Фунтов К. О.; V. A. Zayakhanov; Заяханов В. А.; K. V. Frolov; Фролов К. В.; M. G. Klenov; Клёнов М. Г.; I. Yu. Bondarenko; Бондаренко И. Ю.; I. S. Lyubutin; Любутин И. С.

doi:10.31857/S003281622302026X

Modernized Liquid Helium-Free Closed-Cycle Cryostat for Mössbauer Research

Authors: Starchikov S.S.¹, Funtov K.O.¹, Zayakhanov V.A.¹, Frolov K.V.¹, Klenov M.G.², Bondarenko I.Y.², Lyubutin I.S.¹
Affiliations:
1. Shubnikov Institute of Crystallography of Federal Scientific Research Centre “Crystallography and Photonics”, Russian Academy of Sciences
2. ООО CryoPribor
Issue: No 3 (2023)
Pages: 130-141
Section: ЛАБОРАТОРНАЯ ТЕХНИКА
URL: https://rjsvd.com/0032-8162/article/view/670530
DOI: https://doi.org/10.31857/S003281622302026X
EDN: https://elibrary.ru/GTURMM
ID: 670530

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Abstract

One of the problems in the use of closed-cycle cryostats for applied and basic scientific research is the transmission of mechanical vibrations to the sample. This is particularly relevant for Mössbauer spectroscopy and optical research methods since vibrations lead to broadening of spectral lines. This paper presents various engineering approaches to reducing mechanical vibrations on a sample in closed-cycle cryostats, in particular for Mössbauer spectroscopy. The broadening of the spectral lines of the reference absorber, α-Fe foil, was analyzed and a comparison of the spectra of a FeBO3 single crystal of high structural quality before and after updating the cryostat was made. The obtained results can be used to develop new cryostats or improve existing ones.

References

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